粉体および粉末冶金
Online ISSN : 1880-9014
Print ISSN : 0532-8799
ISSN-L : 0532-8799
研究論文
超微粒超硬合金の抗折力および限界強度に及ぼす破壊の起源となる欠陥寸法およびそれら欠陥の相互作用の影響
徳本 啓高田 真之堤 友浩寺坂 宗太
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ジャーナル オープンアクセス

2024 年 71 巻 9 号 p. 400-408

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Using ultrafine WC powders with different impurities contents, WC-10%Co ultrafine-grained cemented carbides with 5-9 mass% VC addition to the Co content were sintered and then HIPed or HIP-RQ (re-sintered with quenching after HIP). Their transverse-rupture strengths were measured, and the relationship between the stress σd acting on the fracture source and its source size 2a was evaluated using σd-1 - a1/2 and σd - A-1/4 (= σd - (2a)-1/2) correlation diagrams. Each cemented carbide had limiting strength which was constant σd when 2a ≦ 10 μm, regardless of 2a, in both diagrams. The limiting strength of σd was varied from 3.20 to 4.04 GPa, depending on the WC powder, VC addition amount, and HIP and HIP-RQ treatment. While the grinding residual stress proposal was unlikely to be the main cause for ultrafine-grained cemented carbide, the defect expansion proposal due to plastic deformation around the defect was able to explain a part of the phenomenon. It was revealed that if the stress applied to the defect varies due to interactions between defects, this could be the cause of the limiting strength phenomenon. By considering this interaction, it is possible to explain phenomena that could not be explained by the previous proposals.

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© 2024 一般社団法人粉体粉末冶金協会

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