SPring-8/SACLA Research Report

SPring-8/SACLA Research Report

Online ISSN : 2187-6886

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Volume 5, Issue 1

SPring-8 Document D2017-002

Displaying 1-34 of 34 articles from this issue

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Section A

Analysis of the Antigen Recognition Mechanism of Anti-paclitaxel Monoclonal Antibody

Kaori Tabata, Shigeki Arai, Hiroyuki Tanaka, Taro Tamada, Satoshi Mori ...

2017Volume 5Issue 1 Pages 1-3
Published: January 31, 2017
Released on J-STAGE: January 15, 2021

DOIhttps://doi.org/10.18957/rr.5.1.1

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High-resolution Crystallography on Dithionite-reduced NADH-cytochrome b₅ Reductase

Kiyofumi Takaba, Kunio Miki, Kazuki Takeda

2017Volume 5Issue 1 Pages 4-7
Published: January 31, 2017
Released on J-STAGE: January 15, 2021

DOIhttps://doi.org/10.18957/rr.5.1.4

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Development of XMCD Detection ESR

Hiroyuki Nojiri, Michael Baker, Satoshi Matsuzawa, Yasuo Narumi, Tetsu ...

2017Volume 5Issue 1 Pages 8-11
Published: January 31, 2017
Released on J-STAGE: January 15, 2021

DOIhttps://doi.org/10.18957/rr.5.1.8

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Surface Structure Analysis of Activated TiO₂ by Pyrrolidinedithiocarbamate

Masaru Shimomura, Hiroshi Ota, Fumihiko Matsui

2017Volume 5Issue 1 Pages 12-14
Published: January 31, 2017
Released on J-STAGE: January 15, 2021

DOIhttps://doi.org/10.18957/rr.5.1.12

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Alteration of Mouse Nasal Airway Surface Mucociliary Transit by Airway Rehydrating Agents

Martin Donnelley, Kaye Morgan, Nigel Farrow, Richard Carnibella, Rhian ...

2017Volume 5Issue 1 Pages 15-19
Published: January 31, 2017
Released on J-STAGE: January 15, 2021

DOIhttps://doi.org/10.18957/rr.5.1.15

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Cystic fibrosis (CF) is a genetic disorder that compromises the ability of the mucociliary transit (MCT) system to clear debris and pathogens from the airways. To directly assess airway health and the effects of treatments we have developed a synchrotron X-ray microscopy method that non-invasively measures the local rate and patterns of MCT behaviour. The aim of this experiment was to determine if our non-invasive local airway health assessment method could identify changes in nasal MCT rate following clinical treatments known to alter MCT.
Experiments were performed on the BL20XU beamline at the SPring-8 Synchrotron in Japan. Mice were anaesthetized, a small quantity of lead sulphide particles were delivered to the nose, and images of the nasal airways were acquired. The nasal airways were treated with hypertonic saline or mannitol to increase surface hydration and change MCT. Custom software was used to locate and track the motion of the lead particles throughout the image sequences, and to calculate individual and bulk MCT rates.
MCT rates increased following both treatments, but due to high variability there were no statistically significant differences in MCT rate between treatments. However, in future studies we hope that the improved sensitivity provided by this technique will allow us to identify useful CF lung disease-modifying therapies.

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Study of Melt-Isothermal Crystallization Phenomenon of Crystalline Polymers by Utilizing a Simultaneous Measurement System of Synchrotron Wide-Angle and Small-Angle X-ray Scatterings and Transmission FTIR Spectra : Application to the Case of Polyoxymethylene

Kohji Tashiro, Sreeniva Kummara, Hiroko Yamamoto, Taiyo Yoshioka, Dais ...

2017Volume 5Issue 1 Pages 20-26
Published: January 31, 2017
Released on J-STAGE: January 15, 2021

DOIhttps://doi.org/10.18957/rr.5.1.20

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Simultaneous measurement of SAXS, WAXD and FTIR spectra has been performed to clarify the hierarchical evolution in the melt-isothermal crystallization of polyoxymethylene. The derived structural change process was found to be almost common to the various kinds of polymers, suggesting a universality of the proposed crystallization mechanism.

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Analysis of Intramolecular Structural Change of Protein Unfolding-Folding Process by Using Resonant X-ray Scattering

Mitsuhiro Hirai, Satoshi Ajito, Kosuke Takahashi, Kazuki Takeuchi, Ryo ...

2017Volume 5Issue 1 Pages 27-31
Published: January 31, 2017
Released on J-STAGE: January 15, 2021

DOIhttps://doi.org/10.18957/rr.5.1.27

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Analysis of Molecular Aggregation States of Liquid Crystals on Patterned Photo-crosslinking Polymer Thin Film by Synchrotron Radiation Microscopic Infrared Spectroscopy

Yuji Higaki, Ryohei Ishige, Takamichi Shinohara, Daigo Kobayashi, Atsu ...

2017Volume 5Issue 1 Pages 32-34
Published: January 31, 2017
Released on J-STAGE: January 15, 2021

DOIhttps://doi.org/10.18957/rr.5.1.32

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Study of Surface Structure of the Cu-doped Topological Insulator Bi₂Se₃

Tetsuroh Shirasawa, Toshio Takahashi

2017Volume 5Issue 1 Pages 35-37
Published: January 31, 2017
Released on J-STAGE: January 15, 2021

DOIhttps://doi.org/10.18957/rr.5.1.35

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Evaluation by HAXPES of the Chemical State of the Components of a Close-packed Array of Bi-metallic (Au-Ag) Nanoparticles on ITO

Francesca Pincella, Yoshiyuki Yamashita, Rosantha Kumara, Anli Yang, T ...

2017Volume 5Issue 1 Pages 38-44
Published: January 31, 2017
Released on J-STAGE: January 15, 2021

DOIhttps://doi.org/10.18957/rr.5.1.38

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Hard X-ray Photoemission Spectroscopy was employed to investigate the elemental composition and chemical state of core-shell bimetallic nanoparticles deposited on a solid substrate. A shift in Au 4f_7/2and Ag 3d_5/2binding energies together with the change in surface elemental composition of the nanoparticles suggests that a low-temperature alloying occurs for bimetallic nanoparticles.

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X‑ray Structural Analysis of Proteins Involved in Signal Transduction

Mitsuo Kuratani, Seiki Baba, Takaho Terada, Toru Sengoku, Yasushi Hiki ...

2017Volume 5Issue 1 Pages 45-47
Published: January 31, 2017
Released on J-STAGE: January 15, 2021

DOIhttps://doi.org/10.18957/rr.5.1.45

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Section B

Skin Residual Stress Measurements by Synchrotron X-ray Diffraction in Non-sensitized 316 Stainless Steel and High Temperature Water Combination

Masashi Watanabe, Toshio Yonezawa, Tetsuo Shoji

2017Volume 5Issue 1 Pages 48-52
Published: January 31, 2017
Released on J-STAGE: January 15, 2021

DOIhttps://doi.org/10.18957/rr.5.1.48

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Study on Local Structure of Small Amounts of Iron Additives in Fuel Cell Electrolytes by Using Nuclear Resonant Scattering

Atsushi Mineshige, Hideki Yoshioka, Ryohei Mori, Norimasa Umesaki, Kyo ...

2017Volume 5Issue 1 Pages 53-56
Published: January 31, 2017
Released on J-STAGE: January 15, 2021

DOIhttps://doi.org/10.18957/rr.5.1.53

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Effect of Small Amounts of Transition Metal Additives on Physical Properties of Ceramics

Atsushi Mineshige, Hideki Yoshioka, Ryohei Mori, Hironori Ofuchi, Nori ...

2017Volume 5Issue 1 Pages 57-61
Published: January 31, 2017
Released on J-STAGE: January 15, 2021

DOIhttps://doi.org/10.18957/rr.5.1.57

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Small Angle X-ray Scattering of Laser-shocked Aluminum Alloys

Yuji Sano, Ryota Kashiwabara, Norihiro Matsuyama, Kentaro Kajiwara, To ...

2017Volume 5Issue 1 Pages 62-66
Published: January 31, 2017
Released on J-STAGE: January 15, 2021

DOIhttps://doi.org/10.18957/rr.5.1.62

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In-Situ XRD Study of Laminated Lithium Ion Batteries

Hiroaki Kaji, Akira Matsuo, Daisuke Harada, Yoshio Katsuya, Masahiko T ...

2017Volume 5Issue 1 Pages 67-70
Published: January 31, 2017
Released on J-STAGE: January 15, 2021

DOIhttps://doi.org/10.18957/rr.5.1.67

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Local Structure Analysis for the Titanium Oxysulfide as an Anode Material for Li Ion Battery with XAFS

Hiroshi Nozaki, Kazuhiko Dohmae, Hideki Oki

2017Volume 5Issue 1 Pages 71-73
Published: January 31, 2017
Released on J-STAGE: January 15, 2021

DOIhttps://doi.org/10.18957/rr.5.1.71

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Study on Detecting Efficiency of 1-D Detector MYTHEN for Developing Powder Diffractometer

Keiichi Osaka, Masugu Sato, Takuya Matsumoto, Toko Hirono, Morihiro Ka ...

2017Volume 5Issue 1 Pages 74-77
Published: January 31, 2017
Released on J-STAGE: January 15, 2021

DOIhttps://doi.org/10.18957/rr.5.1.74

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Visualization of the Freezing Phenomena in Micro Porous Media by Using X-ray Tomography below the Freezing Point

Tadafumi Daitoku

2017Volume 5Issue 1 Pages 78-83
Published: January 31, 2017
Released on J-STAGE: January 15, 2021

DOIhttps://doi.org/10.18957/rr.5.1.78

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Effect of Cr on Formation of Al₂O₃ Scale Formed on Austenitic Fe-Ni-Cr-Al Alloys

Shigenari Hayashi, Suzue Yoneda, Isao Saeki, Takashi Doi, Daiki Kudo, ...

2017Volume 5Issue 1 Pages 84-87
Published: January 31, 2017
Released on J-STAGE: January 15, 2021

DOIhttps://doi.org/10.18957/rr.5.1.84

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Development of a Method for Measuring Porosity for Aluminum Nitride Coatings by Low Temperature High Velocity Oxygen Fuel Spraying

Yuichi Takahashi, Kazushige Ishida, Takahito Kawai, Ryoichi Yamamoto, ...

2017Volume 5Issue 1 Pages 88-91
Published: January 31, 2017
Released on J-STAGE: January 15, 2021

DOIhttps://doi.org/10.18957/rr.5.1.88

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Observation of Silica-filled Rubber Using Simultaneous Measurement of Time-resolved Ultra-small Angle X-ray Scattering and Viscoelastic Properties

Satoshi Mihara, Naoya Amino, Yuki Sugawara, Shotaro Nishitsuji, Mikihi ...

2017Volume 5Issue 1 Pages 92-96
Published: January 31, 2017
Released on J-STAGE: January 15, 2021

DOIhttps://doi.org/10.18957/rr.5.1.92

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Investigation of the Depth Profile of Constituent Distribution in the Passive Films of the Ni-base Alloy by Hard X-ray Photoemission Spectroscopy

Takashi Doi, Masugu Sato, Hiroshi Oji

2017Volume 5Issue 1 Pages 97-99
Published: January 31, 2017
Released on J-STAGE: January 15, 2021

DOIhttps://doi.org/10.18957/rr.5.1.97

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Investigation on Alteration of Hardened Cement Material due to Elevated Temperature by Non-Destructive Integrated CT-XRD Method

Takafumi Sugiyama, Jhutan Chandra Kuri

2017Volume 5Issue 1 Pages 100-104
Published: January 31, 2017
Released on J-STAGE: January 15, 2021

DOIhttps://doi.org/10.18957/rr.5.1.100

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Analysis on Elemental Form for Biomass Sample

Satoru Hira, Atsushi Ueda, Kenji Suzuki, Ryuji Takeda, Chiya Numako

2017Volume 5Issue 1 Pages 105-109
Published: January 31, 2017
Released on J-STAGE: January 15, 2021

DOIhttps://doi.org/10.18957/rr.5.1.105

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In situ Residual Stress Analysis in Thermosetting Resins for Semiconductor Packaging Substrate during Curing Process for Investigation of their Optimum Thermal Process

Midori Wakabayashi, Atsushi Izumi, Sakiko Suzuki, Toshiaki Watanabe, H ...

2017Volume 5Issue 1 Pages 110-114
Published: January 31, 2017
Released on J-STAGE: January 15, 2021

DOIhttps://doi.org/10.18957/rr.5.1.110

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Analysis of Spatial Inhomogeneity of Residual Stress at Interface between Substrate Resins and Copper Foils in Semiconductor Packaging Substrates

Midori Wakabayashi, Atsushi Izumi, Sakiko Suzuki, Toshiaki Watanabe, H ...

2017Volume 5Issue 1 Pages 115-118
Published: January 31, 2017
Released on J-STAGE: January 15, 2021

DOIhttps://doi.org/10.18957/rr.5.1.115

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Cs Removal Mechanism by Using Aqueous Sodium Metasilicate

Yomei Tokuda, Yoshikatsu Ueda, Hiroshi Goto

2017Volume 5Issue 1 Pages 119-123
Published: January 31, 2017
Released on J-STAGE: January 15, 2021

DOIhttps://doi.org/10.18957/rr.5.1.119

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In Situ Residual Stress Analysis in Resins for Semiconductor Packaging during Curing Process with 2D Detector

Midori Wakabayashi, Atsushi Izumi, Takeshi Kakara, Dai Nagashima, Tosh ...

2017Volume 5Issue 1 Pages 124-127
Published: January 31, 2017
Released on J-STAGE: January 15, 2021

DOIhttps://doi.org/10.18957/rr.5.1.124

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In-situ SAXS Study on Relationship between Structure Change of Aggregates of Fillers in Rubber Materials under Vibration State

Shigeaki Takamatsu, Takashi Yajima, Katsuhiro Yamamoto

2017Volume 5Issue 1 Pages 128-133
Published: January 31, 2017
Released on J-STAGE: January 15, 2021

DOIhttps://doi.org/10.18957/rr.5.1.128

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Three-dimensional Internal Structure Analysis of the Coal/Coke by X-rays Imaging

Katsuhiro Nishihara, Shohki Hatanaka, Reiko Murao, Hideyuki Hayashizak ...

2017Volume 5Issue 1 Pages 134-137
Published: January 31, 2017
Released on J-STAGE: January 15, 2021

DOIhttps://doi.org/10.18957/rr.5.1.134

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Elucidation of Absorption Structure Change on Oil-mineral Interface by Adding Salt for Enhanced Oil Recovery

Sumihiko Murata, Yu Tateyama, Shumpei Sugiyama, Reina Muramatsu, Naoki ...

2017Volume 5Issue 1 Pages 138-140
Published: January 31, 2017
Released on J-STAGE: January 15, 2021

DOIhttps://doi.org/10.18957/rr.5.1.138

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In-situ Residual Stress Analysis in Resins for Semiconductor Packaging during Curing Process with 2D Detector, Part 2

Midori Wakabayashi, Atsushi Izumi, Takeshi Kakara, Dai Nagashima

2017Volume 5Issue 1 Pages 141-144
Published: January 31, 2017
Released on J-STAGE: January 15, 2021

DOIhttps://doi.org/10.18957/rr.5.1.141

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Structural Analysis of Titanium Ion in Sulfuric Acid Solutions by XAFS

Tatsuya Tsurumura, Kazunori Yagi, Yasuo Kameda

2017Volume 5Issue 1 Pages 145-148
Published: January 31, 2017
Released on J-STAGE: January 15, 2021

DOIhttps://doi.org/10.18957/rr.5.1.145

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