Netsu Sokutei
Online ISSN : 1884-1899
Print ISSN : 0386-2615
ISSN-L : 0386-2615
Review
Development of a Top-Loading Type Adiabatic Calorimeter with a Refrigerator
Itaru Tsukushi Eri NishiyamaJun FujimuraMarika Yokota
Author information
JOURNAL FREE ACCESS

2015 Volume 42 Issue 4 Pages 130-134

Details
Abstract
We have developed a top-loading type adiabatic calorimeter with a refrigerator, which works in the temperature range 20–300 K. This calorimeter has following four features, 1) no uses liquid nitrogen and liquid helium for refrigerant, 2) enables us to measure the heat capacities and enthalpy relaxations under stable state for a long time at lower temperature region ( < 77 K: liquid nitrogen temperature), 3) reduces the time required for the sample setup (within ~ 10 min) 4) enables us to set up samples at liquid nitrogen temperature (77 K). The heat capacity of an empty cell was measured in a test experiment. The imprecision of the heat capacity measurement was ±0.8 % at 20–30 K, ±0.4 % at 30–120 K, and ±0.2 % at above 120 K in the present.
Content from these authors
© 2015 The Japan Society of Calorimetry and Thermal Analysis
Next article
feedback
Top