Journal of the Japan Society of Powder and Powder Metallurgy
Online ISSN : 1880-9014
Print ISSN : 0532-8799
ISSN-L : 0532-8799
Solid State Reaction in Mechanically Alloyed Magnesium with Addition of Low-Melting-Metal Oxides
Akihiro YamazakiJunichi KanekoMakoto Sugamata
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JOURNAL OPEN ACCESS

2001 Volume 48 Issue 5 Pages 397-403

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Abstract
Pure magnesium powders were mechanically alloyed with addition powders of low-melting-metal oxides (SnO2, PbO and Sb2O3) by using a planetary ball mill under an Ar atmosphere. After mechanical alloying, the powders were consolidated to the P/M materials by vacuum hot pressing. Solid state reaction in the mechanically alloyed powders and the P/M materials was studied by XRD and DSC. In these systems, the solid state reaction started to occur during MA processing between Mg and low-melting-metal oxides. The added low-melting metal oxides decomposed and formation of MgO and intermetallic compounds (Mg2Sn, Mg2Pb, Mg3Sb2) occurred. Such solid state reaction further progressed during hot-pressing and subsequent heat treatment. Microstructures were studied by TEM and mechanical strength was discussed by hardness values for both MA powders and P/M materials.
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