Journal of the Japan Society of Powder and Powder Metallurgy
Online ISSN : 1880-9014
Print ISSN : 0532-8799
ISSN-L : 0532-8799
High-Temperature Strength of Molybdenum Sheets with Elongated Coarse-Grain Structures
Tomohiro TakidaTadashi IgarashiIsao MutohTatsuhiko Tanabe
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JOURNAL OPEN ACCESS

1999 Volume 46 Issue 5 Pages 489-495

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Abstract
Molybdenum sheets with two types of elongated coarse-grain structures (trade name: TEM) were developed by heavy-duty rolling and recrystallization treatment of sintered molybdenum bodies with 1mass% La2O3. One type of sheets has spindle-like grains (S-TEM), and the other has stacked, plate-like grains (P-TEM). Tensile tests were carried out on S-TEM and P-TEM at 1470K to 2070K in vacuum to investigate the effects of grain structure on tensile properties such as proof strength (σy), tensile strength (σm) and uniform elongation (δm) at high temperatures. The aspect ratio (LTD/W, LRD/W) of grains, i.e., ratio of grain length (L) to grain width (W) on the transverse plane and perpendicular plane to the rolling direction, were estimated as a parameter of grain structure. The following results were obtained.
(1) TEM with elongated coarse-grain structures (S-TEM and P-TEM) had a higher σy and σm than pure molybdenum and TZM with equiaxial-grain structures. At 2070K, the σy and σm of TEM were 2-3 times those of pure molybdenum.
(2) The σy and σm of TEM increased with increased LTD/W, and strain hardening was difficult to perform with increased LRD/W.
(3) Three distinct failure modes were found. The higher the test temperature, the smaller the reduction area in the case of S-TEM with small LTD/W grains. In P-TEM with large LTD/W grains, the reduction was not dependent on temperature, although P-TEM indicated a larger reduction compared to S-TEM. In pure molybdenum and TZM, the higher the test temperature, the larger the reduction.
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