Journal of the Japan Society of Powder and Powder Metallurgy
Online ISSN : 1880-9014
Print ISSN : 0532-8799
ISSN-L : 0532-8799
TiC/SiC Ceramic Composite Prepared by SHS/HP Processing
Toshihiko NishidaKazuya YamadaHiromi NakanoKazuyori Urabe
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JOURNAL OPEN ACCESS

1994 Volume 41 Issue 1 Pages 38-42

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Abstract
Mixtures of Ti-C and Si-C powders respectively equimolar were mixed in various ratios. The final mixture was molded by using an pressure-resistant metallic mold whose inner wall was covered with a carbon felt for insulation. The molded mixture, once set in the mold, was ignited by a tungsten heater and, then, instantaneously uniaxially compressed of 1 GPa (SHS/HP processing). SEM and TEM observations were carried out to get insight in the microstructures obtained for the TiC/SiC composites. Two separated phases, namely SiC and TiC, were present in the composites prepared from Ti-C rich mixtures. In these cases, aggregates of SiC grains, often including some large pores, were found surrounded by the bulk polycrystalline TiC body. On the other hand, fine dispersions of TiC and SiC grains were obtained when nearly equimolar mixtures of Ti-C/Si-C were employed. In this latter case, a maximum value of 28 GPa for the Vickers hardness was measured.
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