Journal of the Japan Society of Powder and Powder Metallurgy
Online ISSN : 1880-9014
Print ISSN : 0532-8799
ISSN-L : 0532-8799
Microstructure of Bi-superconducting Ceramics Prepared by Hot-forge Processing
Toshihiko NishidaSusumu ShimanoKazuyori Urabe
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JOURNAL OPEN ACCESS

1992 Volume 39 Issue 5 Pages 397-400

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Abstract
Bi2Sr2CaCu2Ox ceramic powder prepared by a solid state reaction was encupslated in SUS304 stainless steel mold with dimensions of 22φ(O.D.) - 10φ(l.D.) x 25mm. The mold was preheated at 840°C for 10 minutes and was hot-forged under uniaxial compressive load.
Many kinds of disordered nanostructure were observed in the hot-forged ceramics by TEM. They were many dislocation lines, micro-fracture and lattice undulation in crystal grains. The disordered structure changed, however, to a polycrystal composed of small recrystallized grains after annealing at 800°C for 1 hour.
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